1,12-Dichlorododecane → Sodium Hydroxide

HRID 1660108Notes

Reaction equation

HRID 1660108 reaction equation
[CH2:1]([C:3]1[CH:9]=[CH:8][C:6]([O-:7])=[CH:5][CH:4]=1)[CH3:2].[Na+:10].Cl[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23]Cl>>[CH2:1]([C:3]1[CH:9]=[CH:8][C:6]([O:7][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][O:7][C:6]2[CH:8]=[CH:9][C:3]([CH2:1][CH3:2])=[CH:4][CH:5]=2)=[CH:5][CH:4]=1)[CH3:2].[OH-:7].[Na+:10]

Participants

4

Reactant 2

HCID 775231,12-DichlorododecaneHCID 23672322Sodium p-ethylphenolate

Product 2

HCID 14798Sodium HydroxideHCID 53795930HCID 53795930, compound

Procedure

1,12-bis (4-ethylphenoxy) dodecane is prepared from sodium 4-ethylphenoxide and 1,12-dichlorododecane, according to the method of Example 1, and sulfonated to the disulfonic acid derivative and neutralized with sodium hydroxide according to the method of Example 2, to afford the disodium sulfonate derivative.

Sources & evidence

ORD record
ord-08439230fa134c5e9c08f0a63023873c
Source dataset
uspto-grants-1981_12
Patent number
US04307078

Reaction notes

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