HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → 2-(3-Phthalimidopropylthio)pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Water ethanol | HCID 19096565 | — |
| Reactant | Bromopropylphthalimide | HCID 21958088 | — |
| Reactant | HCID 178418793 | HCID 178418793 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(3-Phthalimidopropylthio)pyrimidine | HCID 3462547 | — |
Reaction Steps
A mixture of 2-mercaptopyrimidine (5.6 g.) and 3-bromopropylphthalimide (13.4 g.) in ethanol (100 ml.) containing sodium (1.15 g.) was heated under reflux for 20 hours affording 2-(3-phthalimidopropylthio)pyrimidine, m.p. 81.5°-82.5° (from ethanol-water).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04307101 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-73aa4fe070874eba80ea616d5e4c5a7a |
| Source note | uspto-grants-1981_12 |