Acrylamide → HCID 86738175, compound

HRID 1660300Notes

Reaction equation

HRID 1660300 reaction equation
[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH2:6]([N:9]([CH2:18][CH:19]=[CH2:20])[CH:10]=[CH:11][CH:12]=[C:13]([C:16]#[N:17])[C:14]#[N:15])[CH:7]=[CH2:8]>C(O)C>[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH2:6]([N:9]([CH:10]=[CH:11][CH:12]=[C:13]([C:14]#[N:15])[C:16]#[N:17])[CH2:18][CH:19]=[CH2:20])[CH:7]=[CH2:8]

Participants

4

Reactant 2

HCID 6579AcrylamideHCID 53724731{3-[Di(prop-2-en-1-yl)amino]prop-2-en-1-ylidene}propanedinitrile

Product 1

HCID 86738175HCID 86738175, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of 40 g. of acrylamide, 52 g. of 3-diallylaminoallylidenemalononitrile (A) in 900 cc. of ethanol was refluxed. 1.3 g. of AZBN was added and the solution refluxed for two hours. At two hour time intervals, the following solutions were added in this order by refluxing:

Workup

  1. additionof AZBN was added
  2. temperaturethe solution refluxed for two hours
  3. additionthe following solutions were added in this order
  4. temperatureby refluxing

Sources & evidence

ORD record
ord-a20e085380b54c7fbce2344106db85a8
Source dataset
uspto-grants-1981_12
Patent number
US04307184

Reaction notes

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