HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1660304Generated: November 2, 2026
N-vinyl-2-pyrrolidone → HCID 86738171, compound
https://huagongshe.com/reaction/1660304
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | N-vinyl-2-pyrrolidone | HCID 6917 | — |
| Reactant | {3-[Di(prop-2-en-1-yl)amino]prop-2-en-1-ylidene}propanedinitrile | HCID 53724731 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 86738171 | HCID 86738171 | — |
Reaction Steps
25 g of intermediate (A) and 25 g of vinylpyrrolidone were dissolved in 100 ml of N-methylpyrrolidone and added with 2.5 g of AZBN. The mixture was then heated to reflux at 85° C. for 6 hours in a flask provided with a stirrer and reflux condenser, then it was cooled, precipitated in ether and dried at 50° C. The yield was 15.7 g of a product soluble in 40:60 water-ethanol, containing about 44% w/w of aminoallylidenmalononitrile moieties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04307183 |
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| Source dataset | uspto-grants-1981_12 |
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| ORD ID | ord-99289c3f4d5e4fb1bdee169b3377c00d |
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| Source note | uspto-grants-1981_12 |
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