{3-[Di(prop-2-en-1-yl)amino]prop-2-en-1-ylidene}propanedinitrile → HCID 131712624, compound

Participants

Reaction Steps

25 g of intermediate (A) and 25 g of vinyloxazolidone were dissolved in 150 ml of ethanol and added with 2.5 g of AZBN. The mixture was heated to reflux for 24 hours in a flask provided with stirrer and reflux condenser. At the end, it was cooled, precipitated in ether, washed and dried. The yield was 14.5 g of a product soluble in water and dimethylformamide, containing about 45% w/w of aminoallylidenmalononitrile moieties.

Provenance & Evidence