HRID1660506
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of 2-(2-fluorophenyl)acetyl chloride (1.73 g, 10 mmole) in dichloromethane (20 ml) was treated with a suspension of sulphur trioxide--dioxane complex (15 mmole) in dichloroethane at 0° C. This mixture was stirred at room temperature for eighteen hours and evaporated to a yellow gum. νmax. (CHCl3) 1805 cm-1.
WORKUP
后处理
- customat 0° C
- customevaporated to a yellow gum