HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfur trioxide → HCID 20556794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfur trioxide | HCID 24682 | — |
| Reactant | 2-(3-chlorophenyl)acetyl Chloride | HCID 10655249 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 20556794 | HCID 20556794 | — |
Reaction Steps
A solution of 3-chlorophenylacetyl chloride (1.89 g, 10 mmole) in dichloromethane (20 ml) was treated with a suspension of sulphur trioxide--dioxane complex (15 mmole) in dichloroethane at 0° C. The mixture was stirred at room temperature for eighteen hours and evaporated, νmax. (CH2Cl2) 1790 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04308259 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-2153ab51fb964532869412e262d766fd |
| Source note | uspto-grants-1981_12 |