HCID 12621985, compound → HCID 178454521, compound

HRID 1660543Notes

Reaction equation

HRID 1660543 reaction equation
[SH:1][C:2]1[NH:7][C:6](=[O:8])[C:5]([CH:9]([NH:11][C:12](=[O:17])[CH2:13][CH:14](C)[CH3:15])[CH3:10])=[N:4][N:3]=1.C(NC(C)C(=O)C(OCC)=O)(=O)CC(C)C>>[SH:1][C:2]1[NH:7][C:6](=[O:8])[C:5]([CH:9]([NH:11][C:12](=[O:17])[CH2:13][CH2:14][CH3:15])[CH3:10])=[N:4][N:3]=1

Participants

3

Reactant 2

HCID 12621985HCID 12621985, compoundHCID 178447346HCID 178447346, compound

Product 1

HCID 178454521HCID 178454521, compound

Procedure

In a similar manner was prepared N-[1-(3-mercapto-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)ethyl]3-methylbutyramide (10.0 g) m.p. 195°-196° (from ethyl acetate) from ethyl 3-isovaleramido-2-oxo-butyrate, thiosemicarbazone (16.56 g).

Sources & evidence

ORD record
ord-5c7998dc6fc540e8bee0525633ef315f
Source dataset
uspto-grants-1981_12
Patent number
US04308384

Reaction notes

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