HCID 136161663, compound → HCID 136059784, compound

HRID 1660544Notes

Reaction equation

HRID 1660544 reaction equation
[CH3:1][S:2][C:3]1[NH:8][C:7](=[O:9])[C:6]([CH:10]([NH:12][C:13](=[O:18])[CH2:14][CH:15](C)[CH3:16])[CH3:11])=[N:5][N:4]=1.SC1NC(=O)C(C(NC(=O)CC(C)C)C)=NN=1>>[CH3:1][S:2][C:3]1[NH:8][C:7](=[O:9])[C:6]([CH:10]([NH:12][C:13](=[O:18])[CH2:14][CH2:15][CH3:16])[CH3:11])=[N:5][N:4]=1

Participants

3

Reactant 2

HCID 136161663HCID 136161663, compoundHCID 178447346HCID 178447346, compound

Product 1

HCID 136059784HCID 136059784, compound

Procedure

In a similar manner was prepared N-[1-(3-methylthio-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)ethyl]-3-methylbutyramide (1.0 g) m.p. 193°-194° (from ethyl acetate) from N-[1-(3-mercapto-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)ethyl]-3-methylbutyramide (2.0 g).

Sources & evidence

ORD record
ord-78298e4ecf2f4b5da893d2058317e61e
Source dataset
uspto-grants-1981_12
Patent number
US04308384

Reaction notes

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