Adipic Acid → HCID 25056529, compound

Participants

Reaction Steps

503 mg of the compound obtained in Example 11 was dissolved in 4 mL of ethyl acetate to which a solution of 183 mg of adipic acid in 3 mL of acetone/water (30/1(v/v)) was then slowly added followed by stirring for 30 min. The reaction mixture was concentrated, to which 2 mL of ethyl acetate and 1 mL of 2-propanol were then added followed by stirring. 15 mL of hexane was added thereto, and resulting mixture was stirred for 10 min and filtered to afford 336 mg of the title compound as a solid.

Provenance & Evidence