HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Trifluoromethyl)benzenesulfonyl chloride → HCID 66789162, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Trifluoromethyl)benzenesulfonyl chloride | HCID 2733250 | — |
| Reactant | HCID 24762630 | HCID 24762630 | — |
| Product | HCID 66789162 | HCID 66789162 | — |
Reaction Steps
4-{[4-(3-Trifluoromethyl-benzenesulfonyl)-3,4-dihydro-2H-benzo[1,4]oxazine-6-carbonyl]-amino}-benzoic acid, MS (ISP): m/e=505.1 (M−H), was prepared as described for example 14, steps 1 to 8. Step 7 was performed using 3-trifluoromethyl-benzenesulfonyl chloride and yielded 4-{[4-(3-trifluoromethyl-benzenesulfonyl)-3,4-dihydro-2H-benzo[1,4]oxazine-6-carbonyl]-amino}-benzoic acid ethyl ester, which was hydrolyzed in step 8.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030308B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-b6e23275418547b8a5ab30922e51a346 |
| Source note | uspto-grants-2011_10 |