5-Amino-3-methyl-1-phenylpyrazole → HCID 67021620, compound
Reaction equation
[N:1]1[C:9]2[C:4](=[N:5][CH:6]=[CH:7][CH:8]=2)[N:3]([C:10]2[CH:15]=[CH:14][C:13]([CH2:16][C:17]([OH:19])=O)=[CH:12][CH:11]=2)[CH:2]=1.[CH3:20][C:21]1[CH:22]=[C:23]([NH2:32])[N:24]([C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)[N:25]=1>>[CH3:20][C:21]1[CH:22]=[C:23]([NH:32][C:17](=[O:19])[CH2:16][C:13]2[CH:12]=[CH:11][C:10]([N:3]3[C:4]4=[N:5][CH:6]=[CH:7][CH:8]=[C:9]4[N:1]=[CH:2]3)=[CH:15][CH:14]=2)[N:24]([C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)[N:25]=1Participants
3
Procedure
The title compound is prepared as described in Example 28 but using 2-(4-imidazo[4,5-b]pyridine-3-yl-phenyl)-acetic acid and 5-methyl-2-phenyl-2H-pyrazol-3-ylamine. Title compound: ES-MS: 409.50 [M+H]+; tR=1.21 min (System 3).
Workup
- customThe title compound is prepared
Sources & evidence
- ORD record
- ord-e640712cfa82412fa88d1a98e9910acb
- Source dataset
- uspto-grants-2011_10
- Patent number
- US08030311B2
Reaction notes
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