HCID 67021570, compound → HCID 67021599, compound

Participants

Reaction Steps

A suspension of [2-methyl-4-(3-nitro-pyridin-2-ylamino)-phenyl]-acetic acid methyl ester (2.2 g, 7.30 mmol) and Raney Ni (˜220 mg) in MeOH (50 mL) is stirred for 6.5 h at rt, under a hydrogen atmosphere. The reaction mixture is filtered through a pad of celite and concentrated to afford the title compound: ES-MS: 272.1 [M+H]+; tR=2.53 min (System 1).

Provenance & Evidence