Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 59233918 | HCID 59233918 | — |
| Product | HCID 59233913 | HCID 59233913 | — |
Reaction Steps
The mixture of 1-(cyanomethyl)-6-chloro-2,3-dihydro-1H-indene-1-carbonitrile (Prep. 39, 250 mg, 1.16 mmol), and AcOH (2.5 ml), H2SO4 (78%, 0.18 ml) was heated to 125° C. The mixture was stirred overnight at 125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08030322B2 |
|---|
| Source dataset | uspto-grants-2011_10 |
|---|
| ORD ID | ord-8ee020e605994996be86f6d60398e7ac |
|---|
| Source note | uspto-grants-2011_10 |
|---|
