HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 136348772, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 52945214 | HCID 52945214 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 136348772 | HCID 136348772 | — |
Reaction Steps
Crystals of ABT-578 ethanol solvate were prepared by adding 417 mg amorphous ABT-578 to a vial and charging 315 mg ethanol 200 proof to it to enable dissolution. This was seeded after 15 hours with the acetonitrile desolvated solvate and incubated at 0 degrees Celsius for an additional 16 hours upon which a crystalline slurry was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030326B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-16eb5ce1c761412d843b408c86b20fcb |
| Source note | uspto-grants-2011_10 |