Thionyl Chloride → HCID 57706274, compound

Participants

Reaction Steps

To a solution of 46.2 (0.164 g, 0.52 mmol) in DCM (5 mL) was added thionyl chloride (76 μL, 1.04 mmol) in one portion at room temperature. The mixture was stirred overnight and concentrated. The crude product was chromatographed on silica gel (0-10% EtOAc/hexane) to afford 46.3 (0.009 g, 5%) as a colorless oil.

Provenance & Evidence