HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 57706368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 57706354 | HCID 57706354 | — |
| Product | HCID 57706368 | HCID 57706368 | 98% |
Reaction Steps
To a flask containing 66.14A (75 mg, 230 μmol) in MeOH (2 mL) was added sulfuric acid (0.61 μL, 11 μmol), and the mixture was stirred at reflux overnight. The reaction was concentrated and then purified by silica gel chromatography (0 to 30% EtOAc/Hexanes) to provide 66.14B (77.0 mg, 98% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030354B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-60bcdfa4f30342b9aeffc43c588145d1 |
| Source note | uspto-grants-2011_10 |