Dimethylformamide → HCID 57706798, compound

Participants

Reaction Steps

To a stirred solution of 66.18F (0.050 g, 0.16 mmol) in DCM (2.00 mL) at 0 C was added DMF (0.0012 mL), followed by thionyl chloride (0.023 mL, 0.32 mmol). The reaction was then stirred for 1.5 hours and then concentrated in vacuo. The product was purified on silica gel (0-10% EtOAc in hexanes) to yield 69.15A as a colorless oil (0.050 g, 94% yield).

Provenance & Evidence