Ethylamine → HCID 67428575, compound

HRID 1662601Notes

Reaction equation

[CH2:1]([O:8][C:9]([N:11]1[CH2:18][CH:17]([F:19])[CH2:16][C@H:12]1[C:13]([OH:15])=O)=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:20]([NH2:22])[CH3:21]>>[CH2:20]([NH:22][C:13]([C@@H:12]1[CH2:16][CH:17]([F:19])[CH2:18][N:11]1[C:9]([O:8][CH2:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1)=[O:10])=[O:15])[CH3:21]

Participants

Reactant 2

HCID 6341Ethylamine

HCID 59996165HCID 59996165, compound

Product 1

HCID 67428575HCID 67428575, compound

Procedure

With 3.02 g of the compound obtained in Step 11-2 and 1.16 g of an aqueous solution of 70% ethyl amine as starting material, 1.92 g of the title compound (colorless solid) was obtained by a similar method to Step 10-1.

Sources & evidence

ORD record: ord-34db6b0e63da4428a9b64aea15655976
Source dataset: uspto-grants-2011_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08030499B2

Reaction notes

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