HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67429188, compound → HCID 11950738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67429188 | HCID 67429188 | — |
| Reactant | 4-Methoxy-2-(trifluoromethoxy)benzene sulfonyl chloride | HCID 86625684 | — |
| Product | HCID 11950738 | HCID 11950738 | — |
Reaction Steps
With 300 mg of the compound obtained in Step 54-1 and 201 mg of 4-methoxy-2-(trifluoromethoxy)benzene sulfonyl chloride as starting materials, 370 mg of free form of the title compound (yellow amorphous) was obtained by a similar method to Example 2. In a similar procedure to Example 43, by subjecting 335 mg of the obtained free form to salt formation and solidification, 314 mg of the title compound (colorless amorphous) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030499B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-9757f724fd1e47788fc452640c5cc482 |
| Source note | uspto-grants-2011_10 |