HRID1662671

反应详情

EQUATION

反应方程式

HRID 1662671 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A suspension of 2.04 g of the compound obtained in Step 82-1 and 0.3 g of 10% palladium-carbon in EtOH (20 ml) was stirred at room temperature for two hours under hydrogen atmosphere. The insoluble matter was separated by filtration and the filtrate was concentrated to obtain 1.05 g of the title compound (pale yellow oil).

WORKUP

后处理

  1. customThe insoluble matter was separated by filtration
  2. concentrationthe filtrate was concentrated