HRID1662671
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
产物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A suspension of 2.04 g of the compound obtained in Step 82-1 and 0.3 g of 10% palladium-carbon in EtOH (20 ml) was stirred at room temperature for two hours under hydrogen atmosphere. The insoluble matter was separated by filtration and the filtrate was concentrated to obtain 1.05 g of the title compound (pale yellow oil).
WORKUP
后处理
- customThe insoluble matter was separated by filtration
- concentrationthe filtrate was concentrated