HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 178503012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | HCID 178508064 | HCID 178508064 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178503012 | HCID 178503012 | — |
Reaction Steps
1 mmol of dimethyl sulphate is added to a mixture of 5 mmol of 3-amino-2-[(E)-pyridin-3-yldiazenyl]-6,7-dihydro-1H,5H-pyrazolo[1,2-a]pyrazol-1-one and 20 ml of THF. The temperature of the medium is brought to 75° C. for 2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08034124B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-628249154243448cb39092940ed0907a |
| Source note | uspto-grants-2011_10 |