HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 58861252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 21096966 | HCID 21096966 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58861252 | HCID 58861252 | — |
Reaction Steps
The process is performed according to the procedure described in Example 3 (step 3.4). Starting with 1.28 g (3.42 mmol) of 3-{2-[1-(6-chloro-2-quinolyl)-4-piperidyl]ethyl}-1,3-oxazolidine-2,4-dione, obtained in step 10.3, and 22.10 ml (154.08 mmol) of a solution (7M) of aqueous ammonia in methanol, and after crystallization from ethanol, 0.64 g of pure product is obtained in the form of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08034818B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-e11fada1432f4dbcbed8a3c9c1f914f0 |
| Source note | uspto-grants-2011_10 |