HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridinecarboxaldehyde → 5-Bromo-2-[(pyridin-4-ylmethyl)-amino]-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | 2-Amino-5-bromobenzoic acid | HCID 79858 | — |
| Product | 5-Bromo-2-[(pyridin-4-ylmethyl)-amino]-benzoic acid | HCID 58989767 | — |
Reaction Steps
Prepared by a similar procedure as described for preparation 1A, starting from 2-amino-5-bromobenzoic acid (Aldrich) and pyridine-4-carbaldehyde. 13C-NMR (DMSO-d6) δ 170.4, 149.4, 149.4, 148.7, 133.9, 132.3, 123.2, 122.0, 112.2, 104.9, 44.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08034811B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-dc60f56f616d4aeca62522ba602d89f3 |
| Source note | uspto-grants-2011_10 |