Anthranilic Acid → HCID 58989854, compound

HRID 1663068Notes

Reaction equation

HRID 1663068 reaction equation
[C:1]([OH:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[NH2:4].[F:11][C:12]1[CH:19]=[CH:18][C:17]([CH:20]=O)=[CH:16][C:13]=1[C:14]#[N:15]>>[C:14]([C:13]1[CH:16]=[C:17]([CH:18]=[CH:19][C:12]=1[F:11])[CH2:20][NH:4][C:3]1[CH:5]=[CH:6][CH:7]=[CH:8][C:2]=1[C:1]([OH:10])=[O:9])#[N:15]

Participants

3

Reactant 2

HCID 227Anthranilic AcidHCID 27695822-Fluoro-5-formylbenzonitrile

Product 1

HCID 58989854HCID 58989854, compound

Procedure

Prepared by a similar procedure as described for preparation 1A, starting from anthranilic acid and 2-fluoro-5-formylbenzonitrile (Aldrich). 13C-NMR (DMSO-d6) δ 172.1, 161.3, 149.5, 138.7, 134.6, 131.9, 130.2, 121.4, 116.6, 114.2, 114.0, 110.0, 99.8, 44.8.

Workup

  1. customPrepared by a similar procedure

Sources & evidence

ORD record
ord-add332ef253c440ca2bef00b074a2933
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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