Anthranilic Acid → HCID 43804238, compound

HRID 1663071Notes

Reaction equation

HRID 1663071 reaction equation
[C:1]([OH:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[NH2:4].[O:11]1[CH2:15][CH2:14][C:13]2[CH:16]=[C:17]([CH:20]=O)[CH:18]=[CH:19][C:12]1=2>>[O:11]1[C:12]2[CH:19]=[CH:18][C:17]([CH2:20][NH:4][C:3]3[CH:5]=[CH:6][CH:7]=[CH:8][C:2]=3[C:1]([OH:10])=[O:9])=[CH:16][C:13]=2[CH2:14][CH2:15]1

Participants

3

Reactant 2

HCID 227Anthranilic AcidHCID 7359012,3-Dihydrobenzofuran-5-carboxaldehyde

Product 1

HCID 43804238HCID 43804238, compound

Procedure

Prepared by a similar procedure as described for preparation 1A, starting from anthranilic acid and 2,3-dihydrobenzo[b]furan-5-carboxaldehyde (Matrix). 13C-NMR (DMSO-d6) δ 169.9, 158.7, 150.6, 134.3, 131.6, 130.9, 127.5, 126.8, 124.0, 114.3, 111.5, 110.1, 108.6, 70.8, 45.6, 29.0.

Workup

  1. customPrepared by a similar procedure

Sources & evidence

ORD record
ord-44583fd7f7064c7ba2ea1dde3ac0c779
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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