Anthranilic Acid → HCID 58990005, compound

HRID 1663072Notes

Reaction equation

HRID 1663072 reaction equation
[C:1]([OH:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[NH2:4].[O:11]1[C:15]2[CH:16]=[CH:17][C:18]([CH:20]=O)=[CH:19][C:14]=2[CH:13]=[CH:12]1>>[O:11]1[C:15]2[CH:16]=[CH:17][C:18]([CH2:20][NH:4][C:3]3[CH:5]=[CH:6][CH:7]=[CH:8][C:2]=3[C:1]([OH:10])=[O:9])=[CH:19][C:14]=2[CH:13]=[CH:12]1

Participants

3

Reactant 2

HCID 227Anthranilic AcidHCID 27738751-Benzofuran-5-carbaldehyde

Product 1

HCID 58990005HCID 58990005, compound

Procedure

Prepared by a similar procedure as described for preparation 1A, starting from anthranilic acid and 1-benzofuran-5-carbaldehyde (Maybridge). 13C-NMR (DMSO-d6) δ 169.9, 153.5, 150.6, 146.3, 134.3, 133.9, 131.6, 127.3, 123.6, 119.5, 114.4, 111.6, 111.2, 110.2, 106.6, 45.8.

Workup

  1. customPrepared by a similar procedure

Sources & evidence

ORD record
ord-10f2442515ed473e851f2fe21b25ae50
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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