Methyl Anthranilate → HCID 58989865, compound

HRID 1663074Notes

Reaction equation

HRID 1663074 reaction equation
C[O:2][C:3](=[O:11])[C:4]1[C:5](=[CH:7][CH:8]=[CH:9][CH:10]=1)[NH2:6].[Cl:12][C:13]1[CH:14]=[N:15][CH:16]=[C:17]([Cl:21])[C:18]=1[CH:19]=O>>[Cl:12][C:13]1[CH:14]=[N:15][CH:16]=[C:17]([Cl:21])[C:18]=1[CH2:19][NH:6][C:5]1[CH:7]=[CH:8][CH:9]=[CH:10][C:4]=1[C:3]([OH:2])=[O:11]

Participants

3

Reactant 2

HCID 8635Methyl AnthranilateHCID 27629883,5-Dichloro-4-pyridinecarboxaldehyde

Product 1

HCID 58989865HCID 58989865, compound

Procedure

Prepared by a similar procedure as described for preparation 1J, starting from anthranilic acid methyl ester and 3,5-dichloro-4-pyridinecarboxaldehyde (Aldrich). 13C-NMR (DMSO-d6) δ 170.1, 149.7, 147.9, 142.6, 133.5, 132.2, 131.7, 115.1, 113.2, 110.9, 41.4.

Workup

  1. customPrepared by a similar procedure

Sources & evidence

ORD record
ord-c75fd467c6674ceab32be2ba1471a0d9
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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