Anthranilic Acid → HCID 178524309, compound

HRID 1663076Notes

Reaction equation

HRID 1663076 reaction equation
[C:1]([OH:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[NH2:4].[OH:11][C:12]1[CH:17]=[C:16]([CH:18]=O)[CH:15]=[CH:14][N:13]=1>>[OH:11][C:12]1[CH:17]=[C:16]([CH2:18][NH:4][C:3]2[CH:5]=[CH:6][CH:7]=[CH:8][C:2]=2[C:1]([OH:10])=[O:9])[CH:15]=[CH:14][N:13]=1

Participants

3

Reactant 2

HCID 227Anthranilic AcidHCID 178519760HCID 178519760, compound

Product 1

HCID 178524309HCID 178524309, compound

Procedure

Prepared by a similar procedure as described for preparation 1A, starting from anthranilic acid and 2-hydroxy-4-pyridinecarboxaldehyde (Tyger). 13C-NMR (DMSO-d6) δ 169.8, 162.4, 153.6, 150.2, 135.0, 134.2, 131.6, 115.8, 114.7, 111.5, 110.5, 104.0, 44.7.

Workup

  1. customPrepared by a similar procedure

Sources & evidence

ORD record
ord-7ae2442bcb414f11a3821c7d82f47def
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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