Anthranilic Acid → HCID 58989959, compound

HRID 1663078Notes

Reaction equation

HRID 1663078 reaction equation
[C:1]([OH:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[NH2:4].[CH3:11][O:12][C:13]1[CH:18]=[CH:17][C:16]([CH:19]=O)=[CH:15][N:14]=1>>[CH3:11][O:12][C:13]1[N:14]=[CH:15][C:16]([CH2:19][NH:4][C:3]2[CH:5]=[CH:6][CH:7]=[CH:8][C:2]=2[C:1]([OH:10])=[O:9])=[CH:17][CH:18]=1

Participants

3

Reactant 2

HCID 227Anthranilic AcidHCID 33645766-Methoxypyridine-3-carbaldehyde

Product 1

HCID 58989959HCID 58989959, compound

Procedure

Prepared by a similar procedure as described for preparation 1A, starting from anthranilic acid and 2-methoxypyridine-5-carboxaldehyde (Aldrich). 13C-NMR (DMSO-d6) δ 169.9, 162.9, 150.4, 145.7, 138.6, 134.4, 131.7, 127.7, 114.7, 111.7, 110.5, 110.5, 53.1, 42.8.

Workup

  1. customPrepared by a similar procedure

Sources & evidence

ORD record
ord-60bf5ff8b8514341bdca3b9cbdb9357e
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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