Methyl Anthranilate → HCID 58989915, compound

HRID 1663079Notes

Reaction equation

HRID 1663079 reaction equation
C[O:2][C:3](=[O:11])[C:4]1[C:5](=[CH:7][CH:8]=[CH:9][CH:10]=1)[NH2:6].[S:12]1[C:16]([CH:17]=O)=[CH:15][N:14]=[CH:13]1>>[S:12]1[C:16]([CH2:17][NH:6][C:5]2[CH:7]=[CH:8][CH:9]=[CH:10][C:4]=2[C:3]([OH:2])=[O:11])=[CH:15][N:14]=[CH:13]1

Participants

3

Reactant 2

HCID 8635Methyl AnthranilateHCID 27735771,3-Thiazole-5-carbaldehyde

Product 1

HCID 58989915HCID 58989915, compound

Procedure

Prepared by a similar procedure as described for preparation 1J, starting from anthranilic acid methyl ester and thiazole-5-carboxaldehyde (Combi-Blocks). 13C-NMR (DMSO-d6) δ 169.8, 153.6, 149.9, 140.8, 137.9, 134.3, 131.6, 115.0, 111.6, 110.7, 38.3.

Workup

  1. customPrepared by a similar procedure

Sources & evidence

ORD record
ord-c883a2d00c1f42d8ba4d7624566a5882
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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