Isatoic Anhydride → HCID 58989867, compound

HRID 1663090Notes

Reaction equation

HRID 1663090 reaction equation
[C:1]12[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=1)[NH:6][C:5](=[O:12])[O:4][C:2]2=[O:3].[N:13]1[CH:18]=[CH:17][C:16]([CH:19](O)[CH3:20])=[CH:15][CH:14]=1>>[N:13]1[CH:18]=[CH:17][C:16]([CH:19]([N:6]2[C:7]3[CH:8]=[CH:9][CH:10]=[CH:11][C:1]=3[C:2](=[O:3])[O:4][C:5]2=[O:12])[CH3:20])=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 8359Isatoic AnhydrideHCID 90919alpha-Methyl-4-pyridinemethanol

Product 1

HCID 58989867HCID 58989867, compound

Procedure

Prepared by a similar procedure as described for preparation 7A, starting from isatoic anhydride and (+/−)-1-(4-pyridyl)ethanol (Fluka). 13C-NMR (DMSO-d6) δ 159.0, 149.8, 148.6, 140.6, 136.5, 129.8, 123.6, 121.2, 115.7, 112.9, 53.1, 15.4.

Workup

  1. customPrepared by a similar procedure

Sources & evidence

ORD record
ord-dec14bfe1f384fca96b988dcde450985
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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