HRID1663090

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8359

2H-3,1-Benzoxazine-2,4(1H)-dione

C8H5NO3

HCID90919

1-(Pyridin-4-yl)ethan-1-ol

C7H9NO

PRODUCTS

产物

HCID58989867

未命名化合物

PROCEDURE

实验过程

Prepared by a similar procedure as described for preparation 7A, starting from isatoic anhydride and (+/−)-1-(4-pyridyl)ethanol (Fluka). 13C-NMR (DMSO-d6) δ 159.0, 149.8, 148.6, 140.6, 136.5, 129.8, 123.6, 121.2, 115.7, 112.9, 53.1, 15.4.

WORKUP

后处理

customPrepared by a similar procedure