N,N-Dimethyl-1,3-propanediamine → HCID 58989972, compound

HRID 1663160Notes

Reaction equation

HRID 1663160 reaction equation
[CH2:1]([O:8][NH:9][C:10]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[NH:18][CH2:19][C:20]1[CH:21]=[CH:22][C:23]([F:29])=[C:24]([CH:28]=1)[C:25](O)=[O:26])=[O:11])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:30][N:31]([CH2:33][CH2:34][CH2:35][NH2:36])[CH3:32]>>[CH2:1]([O:8][NH:9][C:10]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[NH:18][CH2:19][C:20]1[CH:21]=[CH:22][C:23]([F:29])=[C:24]([CH:28]=1)[C:25]([NH:36][CH2:35][CH2:34][CH2:33][N:31]([CH3:32])[CH3:30])=[O:26])=[O:11])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 7993N,N-Dimethyl-1,3-propanediamineHCID 58989938HCID 58989938, compound

Product 1

HCID 58989972HCID 58989972, compound

Procedure

Prepared by a similar procedure as described for the preparation of Example 499, starting from 5-[(2-benzyloxycarbamoyl-phenylamino)methyl]-2-fluoro-benzoic acid (Example 498) and 3-(N,N-dimethylamino)-1-propylamine.

Workup

  1. customPrepared by a similar procedure
  2. customas described for the preparation of Example 499

Sources & evidence

ORD record
ord-fd59ea040c864f73a1e5c3d7a4f35786
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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