HCID 23627639, compound → HCID 67435853, compound

HRID 1663246Notes

Reaction equation

[Cl:1][C:2]1[CH:3]=[C:4]([S:9]([N:12]2[CH:25]([CH2:26][C:27]([OH:29])=O)[C:24]3[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=3)[C:18]3[CH:17]=[CH:16][CH:15]=[CH:14][C:13]2=3)(=[O:11])=[O:10])[CH:5]=[CH:6][C:7]=1[Cl:8].[NH:30]1[CH2:34][CH2:33][N:32]=[C:31]1[C:35]1[CH:47]=[CH:46][C:38]([CH2:39][CH:40]2[CH2:45][CH2:44][NH:43][CH2:42][CH2:41]2)=[CH:37][CH:36]=1>>[Cl:1][C:2]1[CH:3]=[C:4]([S:9]([N:12]2[CH:25]([CH2:26][C:27]([N:43]3[CH2:44][CH2:45][CH:40]([CH2:39][C:38]4[CH:37]=[CH:36][C:35]([C:31]5[NH:32][CH2:33][CH2:34][N:30]=5)=[CH:47][CH:46]=4)[CH2:41][CH2:42]3)=[O:29])[C:24]3[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=3)[C:18]3[CH:17]=[CH:16][CH:15]=[CH:14][C:13]2=3)(=[O:11])=[O:10])[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

Reactant 2

HCID 23627639HCID 23627639, compound

HCID 67436512HCID 67436512, compound

Product 1

HCID 67435853HCID 67435853, compound

Procedure

The title compound was prepared from [5-(3,4-dichloro-benzenesulfonyl)-5,6-dihydro-phenanthridin-6-yl]-acetic acid (Example 2c) and 4-[4-(4,5-dihydro-1H-imidazol-2-yl)-benzyl]-piperidine (Reference Example 6) according to the method described in Example 1e. MS (EI) 674.3 (MH+).

Sources & evidence

ORD record: ord-58a8d368e11f4043aabf1a0121d8a218
Source dataset: uspto-grants-2011_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08034827B2

Reaction notes

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