HCID 67437272, compound → HCID 67435850, compound

Participants

Reaction Steps

To a solution of 4-[(2-{2-[5-(3,4-dichloro-benzenesulfonyl)-5,6-dihydro-phenanthridin-6-yl]-acetylamino}-acetylamino)-methyl]-piperidine-1-carboxylic acid tert-butyl ester (140 mg, 0.2 mmol) in ethyl acetate (5 mL) 2.4M hydrogen chloride in ethyl acetate (4 mL, 9.6 mmol) was added. The reaction mixture was stirred at room temperature overnight, then diluted with diethyl ether (25 mL). The precipitated product was filtered off and washed with diethyl ether to yield 127 mg (87%) of the title compound as white crystals. MS (EI) 602.2 (MH+).

Provenance & Evidence