HCID 67217405, compound → HCID 67436693, compound

HRID 1663258Notes

Reaction equation

HRID 1663258 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([S:9]([N:12]2[CH:25]([CH2:26][C:27](O)=[O:28])[C:24]3[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=3)[C:18]3[CH:17]=[CH:16][CH:15]=[CH:14][C:13]2=3)(=[O:11])=[O:10])=[CH:5][CH:4]=1.[ClH:30].Cl.[NH:32]1[CH2:36][CH2:35][N:34]=[C:33]1[C:37]1[CH:42]=[CH:41][C:40]([CH2:43][CH2:44][NH2:45])=[CH:39][CH:38]=1>>[ClH:30].[NH:34]1[CH2:35][CH2:36][N:32]=[C:33]1[C:37]1[CH:38]=[CH:39][C:40]([CH2:43][CH2:44][NH:45][C:27](=[O:28])[CH2:26][CH:25]2[C:24]3[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=3)[C:18]3[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=3[N:12]2[S:9]([C:6]2[CH:7]=[CH:8][C:3]([O:2][CH3:1])=[CH:4][CH:5]=2)(=[O:11])=[O:10])=[CH:41][CH:42]=1

Participants

3

Reactant 2

HCID 67217405HCID 67217405, compoundHCID 67438554HCID 67438554, compound

Product 1

HCID 67436693HCID 67436693, compound

Procedure

The title compound was prepared from [5-(4-methoxy-benzenesulfonyl)-5,6-dihydro-phenanthridin-6-yl]-acetic acid and 2-[4-(4,5-dihydro-1H-imidazol-2-yl)-phenyl]-ethylamine dihydrochloride (Reference Example 2) according to the method described in Example 1e. MS (EI) 581.6 (MH+).

Sources & evidence

ORD record
ord-c6300ab590024d3189906a86cce3b3df
Source dataset
uspto-grants-2011_10
Patent number
US08034827B2

Reaction notes

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