HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1663378Generated: October 30, 2026
Potassium Carbonate → HCID 86625160, compound
https://huagongshe.com/reaction/1663378
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzene, 1-(bromomethyl)-3-nitro- | HCID 77568 | — |
| Reactant | HCID 86062035 | HCID 86062035 | — |
| Catalyst | Tetrabutylammonium Iodide | HCID 67553 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86625160 | HCID 86625160 | — |
Reaction Steps
A mixture of 3-bromo-5-formyl-2-hydroxy-benzoic acid methyl ester (518 mg), potassium carbonate (613 mg), tetrabutylammonium iodide (68 mg) and 3-nitrobenzyl bromide (525 mg) in DMF (10 ml) was heated at 60° C. for 5 h. The mixture was diluted with water and extracted with ethyl acetate. The organic layer was dried (MgSO4), filtered and concentrated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08034945B2 |
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| Source dataset | uspto-grants-2011_10 |
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| ORD ID | ord-eed86f49a7c94bd99d15463c58bdbeb6 |
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| Source note | uspto-grants-2011_10 |
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