HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 57505493, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1H-Benzimidazol-5-ol,1,2-dimethyl-(9CI) | HCID 658535 | — |
| Reactant | N-(6-iodoimidazo[1,2-b]pyridazin-2-yl)cyclopropanecarboxamide | HCID 57386058 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 57505493 | HCID 57505493 | 28.2% |
Reaction Steps
Using N-(6-iodoimidazo[1,2-b]pyridazin-2-yl)cyclopropanecarboxamide (254 mg, 0.774 mmol), 1,2-dimethyl-1H-benzimidazole-5-ol (163 mg, 1.06 mmol), potassium carbonate (267 mg, 1.94 mmol) and N,N-dimethylformamide (3.0 mL) as starting materials and in the same manner as in Example 95, the title compound (79 mg, 28%) was obtained as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08034812B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-c5673d639e654f7e91bd27632884d7ab |
| Source note | uspto-grants-2011_10 |