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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1663782Generated: October 30, 2026

Hydroxybenzenesulfonic acid → HCID 86630643, compound

https://huagongshe.com/reaction/1663782

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxybenzenesulfonic acidHCID 15619088—
ReactantTak-593HCID 24767976—
SolventEthanolHCID 702—
ProductHCID 86630643HCID 8663064375%

Reaction Steps

Using N-[5-({2-[(cyclopropylcarbonyl)amino]imidazo[1,2-b]pyridazin-6-yl}oxy)-2-methylphenyl]-1,3-dimethyl-1H-pyrazole-5-carboxamide (2.00 g, 4.49 mmol), ethanol (100 mL) and benzenesulfonic acid monohydrate (0.83 g, 4.71 mmol), and in the same manner as in Example 152, the title compound (2.02 g, 75%) was obtained as white crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08034812B2
Source datasetuspto-grants-2011_10
ORD IDord-4f5b263061ff4e71a626e8bbd6bf718f
Source noteuspto-grants-2011_10