Ethylorthoformate → HCID 57600223, compound

Participants

Reaction Conditions

Reaction Steps

The mixture of (2E)-3-butyl-3,7-dihydro-1H-purine-2,6-dione 2-hydrazone (200 mg, 0.0009 mol) in Ethyl orthoformate (5 mL, 0.03 mol) was heated at 100° C. overnight. After cooling to room temperature, the reaction mixture was filtrated and dried to give the desired product (150 mg, 71.8%). LCMS calculated for C10H13N6O (M+H): 233.1. found: 233.1.

Provenance & Evidence