HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 178446139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | HCID 178446164 | HCID 178446164 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178446139 | HCID 178446139 | — |
Reaction Steps
A solution of (2E)-3-pentyl-3,7-dihydro-1h-purine-2,6-dione 2-hydrazone (104 mg, 44 μmol), benzaldehyde (44.7 μl, 44 μmol) in ethanol (10 ml) was stirred at 70° C. for 3 hours. The reaction solution was concentrated in vacuo to give the desired product. LCMS calculated for C17H21N6O (M+H): 325.2. found: 325.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08039478B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-89aea5b11e4446c7ae07bb096d73fd5e |
| Source note | uspto-grants-2011_10 |