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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1664587Generated: October 29, 2026

HCID 57600319, compound → HCID 57600282, compound

https://huagongshe.com/reaction/1664587

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57600319HCID 57600319—
SolventHydrochloric AcidHCID 313—
SolventTetrahydrofuranHCID 8028—
ProductHCID 57600282HCID 57600282—

Reaction Steps

A mixture of 3-(3,3-diethoxypropyl)-5-(4-methoxyphenyl)-1,2,4-oxadiazole (1.0 g, 3.0 mmol) in 2N HCl (10 mL) and THF (10 mL) was stirred at room temperature overnight. The reaction mixture was extracted with EtOAc (3×). The organic layers were washed with water, dried over Na2SO4, filtered and concentrated to give the desired product. LCMS calculated for C12H13N2O3 (M+H): 233.1. found: 233.1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08039478B2
Source datasetuspto-grants-2011_10
ORD IDord-283e8714dd3f49c3b4bba5122d9035d6
Source noteuspto-grants-2011_10