Benzyl (3-Oxopropyl)carbamate → HCID 178446144, compound

Participants

Reaction Steps

A mixture of (2E)-3-pentyl-3,7-dihydro-1H-purine-2,6-dione 2-hydrazone (2.3 g, 9.6 mmol) and benzyl (3-oxopropyl)carbamate (2.0 g, 9.6 mmol) in ethanol (30 mL) was refluxed overnight. The reaction mixture was concentrated to give the product (4.0 g, 58% yield), which was used for next step without further purification. LCMS calculated for C21H28N7O3 (M+H): 426.2. found: 426.1.

Provenance & Evidence