huagongshe.com
HRID1664687

反应详情

EQUATION

反应方程式

HRID 1664687 的结构方程式

REACTANTS

反应物

1
结构：Cc1cc([N+](=O)[O-])c(OC(C)C)cc1C1=CCC(N(C)C)CC1
HCID59764470

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(N)c(OC(C)C)cc1C1CCC(N(C)C)CC1
HCID59764590

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

To a solution of 4-(5-isopropoxy-2-methyl-4-nitrophenyl)-N,N-dimethylcyclohex-3-enamine (0.1 mmol) in 10 mL of MeOH, is added Pd/C (5 mg) under argon. The suspension is stirred under 1 atm. H2 for 6 hours. After filtering, solvent is removed and 4-(4-(dimethylamino)cyclohexyl)-2-isopropoxy-5-methylaniline is obtained. MS (ES+): 291.24 (M+1)+.

WORKUP

后处理

  1. filtrationAfter filtering
  2. customsolvent is removed