HCID 67438660, compound → HCID 59722552, compound

Participants

Reaction Steps

Palladium (10% on carbon; 0.50 g) was added to a solution of benzyl 4-(3-oxo-6-phenyl-2,3-dihydropyridazin-4-yl)piperidine-1-carboxylate (1.10 g, 2.82 mmol) in ethanol (50 mL). The reaction vessel was evacuated and back-filled with nitrogen (3×), then back-filled with hydrogen (1 atm). After 24 h, the mixture was filtered through celite and concentrated to give the title compound (709 mg). MS 256.2 (M+1).

Provenance & Evidence