HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium carbonate → HCID 25234316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | HCID 67438422 | HCID 67438422 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 25234316 | HCID 25234316 | — |
Reaction Steps
In analogy to example 10, step 3, propane-2-sulfonic acid (3′-methanesulfonyl-biphenyl-3-ylmethyl)-amide was reacted with 1-iodopropane and cesium carbonate in N,N-dimethylacetamide to give propane-2-sulfonic acid (3′-methanesulfonyl-biphenyl-3-ylmethyl)-propyl-amide as a colorless, waxy solid. MS: 427.2 ([M+NH4]+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08039493B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-f8911af4d8cf486e93204656836f462a |
| Source note | uspto-grants-2011_10 |