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HRID1665270

反应详情

EQUATION

反应方程式

HRID 1665270 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)[C@@H]1CCCC[C@H]1C(=O)O
HCID720895

未命名化合物

结构：O=C1C(=O)c2ccccc2C2=C1SCC1(CCNCC1)O2
HCID57661820

Spiro[naphtho[1,2-b]-1,4-oxathiin-2(3H),4′-piperidine]-5,6-dione

C16H15NO3S

PRODUCTS

生成物

1
结构：O=C([O-])[C@@H]1CCCC[C@H]1C(=O)O.O=C1C(=O)c2ccccc2C2=C1SCC1(CC[NH2+]CC1)O2
HCID131729238

未命名化合物

PROCEDURE

实验过程

Compound 15 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, trans-cyclohexane-1,2-dicarboxylic acid and conditions outlined for compound 14. M.p.=208-211° C.; 400 MHz 1H NMR (DMSO-d6) δ: 7.90-7.87 (m, 1H), 7.82-7.73 (m, 2H), 7.58-7.53 (m, 1H), 3.06 (s, 2H), 2.96-2.86 (m, 4H), 2.29-2.26 (m, 2H), 1.98-1.91 (m, 4H), 1.77-1.65 (m, 4H), 1.23-1.17 (m, 4H); LCMS: 302 [M+H].