(Phenylthio)acetyl chloride → HCID 57661976, compound

Participants

Reaction Steps

Compound 48 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, (phenylthio)acetyl chloride and conditions outlined in procedure N. M.p.=155-157° C.; 300 MHz 1H NMR (DMSO-d6) δ 7.89 (m, 2H), 7.76 (t, 1H), 7.60 (t, 1H), 7.39 (m, 2H), 7.29 (m, 2H), 7.20 (m, 1H), 4.11 (dd, 2H), 4.05 (s, 2H), 3.42 (t, 2H), 3.11 (s, 2H), 2.05 (m, 2H), 1.80 (m, 2H); LCMS: 452 [M+H].

Provenance & Evidence