HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloro(phenyl)acetyl chloride → HCID 57661957, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloro(phenyl)acetyl chloride | HCID 102902 | — |
| Reactant | Spiro[naphtho[1,2-b][1,4]oxathiine-2,4'-piperidine]-5,6-dione | HCID 57661820 | — |
| Product | HCID 57661957 | HCID 57661957 | — |
Reaction Steps
Compound 50 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, chloro(phenyl)acetyl chloride and conditions outlined in procedure N. M.p.=125-126° C.; 300 MHz 1H NMR (DMSO-d6) δ 7.62-7.88 (m, 3H), 7.35-7.55 (m, 6H), 6.44 (d, 1H), 4.15 (m, 2H), 3.30 (m, 2H), 3.0-3.13 (2s, 2H), 2.0 (m, 2H), 1.65 (m, 2H); LCMS: 454 [M+H].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08039503B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-908823493172456e844c4e27c4736613 |
| Source note | uspto-grants-2011_10 |