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HRID1665289

反应详情

EQUATION

反应方程式

HRID 1665289 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)c1cccc(C(F)(F)F)c1
HCID75257

Benzoyl chloride, 3-(trifluoromethyl)-

C8H4ClF3O

结构：O=C1C(=O)c2ccccc2C2=C1SCC1(CCNCC1)O2
HCID57661820

Spiro[naphtho[1,2-b]-1,4-oxathiin-2(3H),4′-piperidine]-5,6-dione

C16H15NO3S

PRODUCTS

生成物

1
结构：O=C1C(=O)c2ccccc2C2=C1SCC1(CCN(C(=O)c3cccc(C(F)(F)F)c3)CC1)O2
HCID57661889

未命名化合物

PROCEDURE

实验过程

Compound 54 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 3-(trifluoromethyl)benzoyl chloride and conditions outlined in procedure N. M.p.=165-166° C.; 300 MHz 1H NMR (DMSO-d6) δ 7.70-7.98 (m, 7H), 7.57 (m, 1H), 4.40 (m, 1H), 3.55 (brm, 2H), 3.30 (m, 1H), 3.11 (s, 2H), 2.10 (m, 1H), 1.85 (m, 3H); LCMS: 474 [M+H].